Development of a certified reference material for the mass concentration of active chlorine in water and its application for an interlaboratory comparison

Verfasser / Beitragende:
[Maria Krasheninina, Maria Medvedevskikh, Anna Sergeeva, Olga Golynets]
Ort, Verlag, Jahr:
2015
Enthalten in:
Accreditation and Quality Assurance, 20/3(2015-06-01), 171-178
Format:
Artikel (online)
ID: 605465738
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024 7 0 |a 10.1007/s00769-015-1124-5  |2 doi 
035 |a (NATIONALLICENCE)springer-10.1007/s00769-015-1124-5 
245 0 0 |a Development of a certified reference material for the mass concentration of active chlorine in water and its application for an interlaboratory comparison  |h [Elektronische Daten]  |c [Maria Krasheninina, Maria Medvedevskikh, Anna Sergeeva, Olga Golynets] 
520 3 |a The article discusses the development of a certified reference material (CRM) of mass concentration of active chlorine in water, GSO 10138-2012, which was performed in the Ural Scientific Research Institute for Metrology (UNIIM), Russia. For this purpose, N-chlorobenzenesulfonamide sodium salt trihydrate (chloramine B) was selected. Identification and purity assessment of the chloramine B reagent were conducted by applying gas chromatography with mass spectrometric detection. The CRM's certified value was determined by oxidation-reduction titration. Its uncertainty was estimated by combining the contributions from characterization, inhomogeneity and instability. The article also presents the results of an interlaboratory comparison in which 42 Russian laboratories participated. 
540 |a Springer-Verlag Berlin Heidelberg, 2015 
690 7 |a Reference materials  |2 nationallicence 
690 7 |a Active chlorine  |2 nationallicence 
690 7 |a Water quality  |2 nationallicence 
690 7 |a Interlaboratory comparison  |2 nationallicence 
700 1 |a Krasheninina  |D Maria  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
700 1 |a Medvedevskikh  |D Maria  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
700 1 |a Sergeeva  |D Anna  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
700 1 |a Golynets  |D Olga  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
773 0 |t Accreditation and Quality Assurance  |d Springer Berlin Heidelberg  |g 20/3(2015-06-01), 171-178  |x 0949-1775  |q 20:3<171  |1 2015  |2 20  |o 769 
856 4 0 |u https://doi.org/10.1007/s00769-015-1124-5  |q text/html  |z Onlinezugriff via DOI 
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900 7 |a Metadata rights reserved  |b Springer special CC-BY-NC licence  |2 nationallicence 
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950 |B NATIONALLICENCE  |P 700  |E 1-  |a Krasheninina  |D Maria  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Medvedevskikh  |D Maria  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Sergeeva  |D Anna  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Golynets  |D Olga  |u Ural Scientific Research Institute for Metrology (UNIIM), Krasnoarmeiskaya St. 4, 620000, Ekaterinburg, Russian Federation  |4 aut 
950 |B NATIONALLICENCE  |P 773  |E 0-  |t Accreditation and Quality Assurance  |d Springer Berlin Heidelberg  |g 20/3(2015-06-01), 171-178  |x 0949-1775  |q 20:3<171  |1 2015  |2 20  |o 769