The question of homogeneity inside a chimney: application of ISO13528 to stack emission proficiency tests

Verfasser / Beitragende:
[Jens Cordes, Benno Stoffels, Dominik Wildanger]
Ort, Verlag, Jahr:
2015
Enthalten in:
Accreditation and Quality Assurance, 20/4(2015-08-01), 287-295
Format:
Artikel (online)
ID: 605465908
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024 7 0 |a 10.1007/s00769-015-1139-y  |2 doi 
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245 0 4 |a The question of homogeneity inside a chimney: application of ISO13528 to stack emission proficiency tests  |h [Elektronische Daten]  |c [Jens Cordes, Benno Stoffels, Dominik Wildanger] 
520 3 |a The Hessian Agency for the Environment and Geology (HLUG) in Kassel, Germany, offers stack emission proficiency tests (PTs) on an in-house-constructed emission simulation apparatus (ESA). The PTs include gaseous (organic and inorganic) and particulate matter (heavy-metal-doped dust) emissions. A unique challenge arises when ISO13528 is applied to these PTs: While homogeneity of the used gases, liquids, and dusts can easily be demonstrated, the equivalence of measurement points along the stack emission chimney is a completely different matter. Since each test item batch (in this case the pollution-doped ESA exhaust gas) only exists during one measurement, the standard procedure for determination of homogeneity (in this case equivalence of the sampling openings) is not applicable to determine compliance to the standard. To demonstrate the equivalence of the measurement points on our ESA, we devised a modified homogeneity check based on ISO13528 annexB. This modified homogeneity check was successfully applied to our stack emission PT and should be applicable to sampling PTs in general. 
540 |a The Author(s), 2015 
690 7 |a Stack emissions  |2 nationallicence 
690 7 |a Proficiency tests  |2 nationallicence 
690 7 |a Sampling  |2 nationallicence 
690 7 |a Homogeneity check  |2 nationallicence 
690 7 |a ISO13528  |2 nationallicence 
690 7 |a ISO17043  |2 nationallicence 
690 7 |a D : Particle diameter  |2 nationallicence 
690 7 |a g : Number of proficiency test items or sampling positions/times tested in a homogeneity check  |2 nationallicence 
690 7 |a m : Number of repeat measurements made per proficiency test item or repeat samplings made per sampling position/time  |2 nationallicence 
690 7 |a q 3( D ) : Quantile of particles with a diameter ≤D  |2 nationallicence 
690 7 |a s : Standard deviation  |2 nationallicence 
690 7 |a s r : Relative standard deviation  |2 nationallicence 
690 7 |a s s : Estimate of between-sample standard deviation  |2 nationallicence 
690 7 |a s rs : Estimate of relative between-sample standard deviation  |2 nationallicence 
690 7 |a s w : Within-sample standard deviation  |2 nationallicence 
690 7 |a s x : Standard deviation of sample averages  |2 nationallicence 
690 7 |a x : Measurement result (e.g., mass concentration)  |2 nationallicence 
690 7 |a $$ \bar{x} $$ x ¯ : General average of x  |2 nationallicence 
690 7 |a σ pt : Standard deviation for proficiency assessment  |2 nationallicence 
700 1 |a Cordes  |D Jens  |u Department I3 - Air Pollution, Emission, HLUG, Hessian Agency for the Environment and Geology, Ludwig-Mond-Straße 33, 34121, Kassel, Germany  |4 aut 
700 1 |a Stoffels  |D Benno  |u Department I3 - Air Pollution, Emission, HLUG, Hessian Agency for the Environment and Geology, Ludwig-Mond-Straße 33, 34121, Kassel, Germany  |4 aut 
700 1 |a Wildanger  |D Dominik  |u Department I3 - Air Pollution, Emission, HLUG, Hessian Agency for the Environment and Geology, Ludwig-Mond-Straße 33, 34121, Kassel, Germany  |4 aut 
773 0 |t Accreditation and Quality Assurance  |d Springer Berlin Heidelberg  |g 20/4(2015-08-01), 287-295  |x 0949-1775  |q 20:4<287  |1 2015  |2 20  |o 769 
856 4 0 |u https://doi.org/10.1007/s00769-015-1139-y  |q text/html  |z Onlinezugriff via DOI 
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900 7 |a Metadata rights reserved  |b Springer special CC-BY-NC licence  |2 nationallicence 
908 |D 1  |a research-article  |2 jats 
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950 |B NATIONALLICENCE  |P 856  |E 40  |u https://doi.org/10.1007/s00769-015-1139-y  |q text/html  |z Onlinezugriff via DOI 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Cordes  |D Jens  |u Department I3 - Air Pollution, Emission, HLUG, Hessian Agency for the Environment and Geology, Ludwig-Mond-Straße 33, 34121, Kassel, Germany  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Stoffels  |D Benno  |u Department I3 - Air Pollution, Emission, HLUG, Hessian Agency for the Environment and Geology, Ludwig-Mond-Straße 33, 34121, Kassel, Germany  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Wildanger  |D Dominik  |u Department I3 - Air Pollution, Emission, HLUG, Hessian Agency for the Environment and Geology, Ludwig-Mond-Straße 33, 34121, Kassel, Germany  |4 aut 
950 |B NATIONALLICENCE  |P 773  |E 0-  |t Accreditation and Quality Assurance  |d Springer Berlin Heidelberg  |g 20/4(2015-08-01), 287-295  |x 0949-1775  |q 20:4<287  |1 2015  |2 20  |o 769