Validation of a GC-IDMS method for the metrologically traceable quantification of selected FAMEs in biodiesel
| LEADER | caa a22 4500 | ||
|---|---|---|---|
| 001 | 605466114 | ||
| 003 | CHVBK | ||
| 005 | 20210128100305.0 | ||
| 007 | cr unu---uuuuu | ||
| 008 | 210128e20151001xx s 000 0 eng | ||
| 024 | 7 | 0 | |a 10.1007/s00769-015-1144-1 |2 doi |
| 035 | |a (NATIONALLICENCE)springer-10.1007/s00769-015-1144-1 | ||
| 245 | 0 | 0 | |a Validation of a GC-IDMS method for the metrologically traceable quantification of selected FAMEs in biodiesel |h [Elektronische Daten] |c [Valle Morales, Ahmet Goren, Andrea Held, Mine Bilsel, Simay Gündüz, Hasibe Yilmaz] |
| 520 | 3 | |a Current methods for the analysis of fatty acid methyl esters (FAMEs) in rapeseed oil-based biodiesel refer to operationally defined measurands, which is a practical solution for routine analysis. In this paper, a new method for the SI-traceable quantification of selected FAMEs in biodiesel and its validation are described. This method has the potential to be a reference method for applications requiring structurally defined measurands and traceability to the SI as it allows direct comparisons to well-characterised calibrants through the use of isotopically labelled analogues of the analytes as well as establishing a full uncertainty budget. The method is based on gas chromatography-isotope dilution mass spectrometry. Its performance is demonstrated through its implementation and validation in two independent laboratories and is shown to provide reliable and traceable results for selected FAMEs in biodiesel test samples. | |
| 540 | |a The Author(s), 2015 | ||
| 690 | 7 | |a Biofuels |2 nationallicence | |
| 690 | 7 | |a Biodiesel |2 nationallicence | |
| 690 | 7 | |a GC-IDMS |2 nationallicence | |
| 690 | 7 | |a Traceability |2 nationallicence | |
| 690 | 7 | |a Fatty acid methyl ester |2 nationallicence | |
| 700 | 1 | |a Morales |D Valle |u Institute for Reference Materials and Measurements, European Commission, Joint Research Centre, Geel, Belgium |4 aut | |
| 700 | 1 | |a Goren |D Ahmet |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | |
| 700 | 1 | |a Held |D Andrea |u Institute for Reference Materials and Measurements, European Commission, Joint Research Centre, Geel, Belgium |4 aut | |
| 700 | 1 | |a Bilsel |D Mine |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | |
| 700 | 1 | |a Gündüz |D Simay |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | |
| 700 | 1 | |a Yilmaz |D Hasibe |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | |
| 773 | 0 | |t Accreditation and Quality Assurance |d Springer Berlin Heidelberg |g 20/5(2015-10-01), 411-419 |x 0949-1775 |q 20:5<411 |1 2015 |2 20 |o 769 | |
| 856 | 4 | 0 | |u https://doi.org/10.1007/s00769-015-1144-1 |q text/html |z Onlinezugriff via DOI |
| 898 | |a BK010053 |b XK010053 |c XK010000 | ||
| 900 | 7 | |a Metadata rights reserved |b Springer special CC-BY-NC licence |2 nationallicence | |
| 908 | |D 1 |a research-article |2 jats | ||
| 949 | |B NATIONALLICENCE |F NATIONALLICENCE |b NL-springer | ||
| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1007/s00769-015-1144-1 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Morales |D Valle |u Institute for Reference Materials and Measurements, European Commission, Joint Research Centre, Geel, Belgium |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Goren |D Ahmet |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Held |D Andrea |u Institute for Reference Materials and Measurements, European Commission, Joint Research Centre, Geel, Belgium |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Bilsel |D Mine |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Gündüz |D Simay |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Yilmaz |D Hasibe |u TÜBİTAK-UME (National Metrology Institute), Gebze-Kocaeli, Turkey |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Accreditation and Quality Assurance |d Springer Berlin Heidelberg |g 20/5(2015-10-01), 411-419 |x 0949-1775 |q 20:5<411 |1 2015 |2 20 |o 769 | ||