The effect of premature wall yield on creep testing of strongly flocculated suspensions

Verfasser / Beitragende:
[Anthony Stickland, Ashish Kumar, Tiara Kusuma, Peter Scales, Amy Tindley, Simon Biggs, Richard Buscall]
Ort, Verlag, Jahr:
2015
Enthalten in:
Rheologica Acta, 54/5(2015-05-01), 337-352
Format:
Artikel (online)
ID: 605466734
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024 7 0 |a 10.1007/s00397-015-0847-x  |2 doi 
035 |a (NATIONALLICENCE)springer-10.1007/s00397-015-0847-x 
245 0 4 |a The effect of premature wall yield on creep testing of strongly flocculated suspensions  |h [Elektronische Daten]  |c [Anthony Stickland, Ashish Kumar, Tiara Kusuma, Peter Scales, Amy Tindley, Simon Biggs, Richard Buscall] 
520 3 |a Measuring yielding in cohesive suspensions is often hampered by slip at measurement surfaces. This paper presents creep data for strongly flocculated suspensions obtained using vane-in-cup tools with differing cup-to-vane diameter ratios. The three suspensions were titania and alumina aggregated at their isoelectric points and polymer-flocculated alumina. The aim was to find the diameter ratio where slip or premature yielding at the cup wall had no effect on the transient behaviour. The large diameter ratio results showed readily understandable material behaviour comprising linear viscoelasticity at low stresses, strain-softening close to yielding, time-dependent yield across a range of stresses and then viscous flow. Tests in small ratio geometries however showed more complex responses. Effects attributed to the cup wall included delayed softening, slip, multiple yielding and stick-slip events, and unsteady flow. The conclusion was that cups have to be relatively large to eliminate wall artefacts. A diameter ratio of three was sufficient in practice, although the minimum ratio must be material dependent. 
540 |a Springer-Verlag Berlin Heidelberg, 2015 
690 7 |a Suspension rheology  |2 nationallicence 
690 7 |a Creep  |2 nationallicence 
690 7 |a Vane-in-cup  |2 nationallicence 
690 7 |a Wall slip  |2 nationallicence 
690 7 |a Strongly flocculated suspension  |2 nationallicence 
700 1 |a Stickland  |D Anthony  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
700 1 |a Kumar  |D Ashish  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
700 1 |a Kusuma  |D Tiara  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
700 1 |a Scales  |D Peter  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
700 1 |a Tindley  |D Amy  |u Institute of Particle Science and Engineering, School of Process, Environmental and Materials Engineering, The University of Leeds, LS2 9JT, Leeds, UK  |4 aut 
700 1 |a Biggs  |D Simon  |u Institute of Particle Science and Engineering, School of Process, Environmental and Materials Engineering, The University of Leeds, LS2 9JT, Leeds, UK  |4 aut 
700 1 |a Buscall  |D Richard  |u MSACT Research and Consulting, 34, Maritime Court, Haven Road, EX2 8GP, Exeter, UK  |4 aut 
773 0 |t Rheologica Acta  |d Springer Berlin Heidelberg  |g 54/5(2015-05-01), 337-352  |x 0035-4511  |q 54:5<337  |1 2015  |2 54  |o 397 
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950 |B NATIONALLICENCE  |P 700  |E 1-  |a Stickland  |D Anthony  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Kumar  |D Ashish  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Kusuma  |D Tiara  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Scales  |D Peter  |u Particulate Fluids Processing Centre, Department of Chemical and Biomolecular Engineering, The University of Melbourne, 3010, Victoria, Australia  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Tindley  |D Amy  |u Institute of Particle Science and Engineering, School of Process, Environmental and Materials Engineering, The University of Leeds, LS2 9JT, Leeds, UK  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Biggs  |D Simon  |u Institute of Particle Science and Engineering, School of Process, Environmental and Materials Engineering, The University of Leeds, LS2 9JT, Leeds, UK  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Buscall  |D Richard  |u MSACT Research and Consulting, 34, Maritime Court, Haven Road, EX2 8GP, Exeter, UK  |4 aut 
950 |B NATIONALLICENCE  |P 773  |E 0-  |t Rheologica Acta  |d Springer Berlin Heidelberg  |g 54/5(2015-05-01), 337-352  |x 0035-4511  |q 54:5<337  |1 2015  |2 54  |o 397