Three-component spiro heterocyclization of 1 H -pyrrole-2,3-diones with acetonitriles and 4-hydroxycoumarin. Crystal and molecular structure of ethyl 2-amino-3-cyano-1′-cyclohexyl-2′,5-dioxo-5′-phenyl-1′,2′-dihydro-5 H -spiro-[pyrano[3,2- c ]chromene-4,3′-pyrrole]-4′-carboxylate

Verfasser / Beitragende:
[M. Dmitriev, P. Silaichev, A. Maslivets]
Ort, Verlag, Jahr:
2015
Enthalten in:
Russian Journal of Organic Chemistry, 51/1(2015-01-01), 74-77
Format:
Artikel (online)
ID: 605528624
LEADER caa a22 4500
001 605528624
003 CHVBK
005 20210128100814.0
007 cr unu---uuuuu
008 210128e20150101xx s 000 0 eng
024 7 0 |a 10.1134/S1070428015010121  |2 doi 
035 |a (NATIONALLICENCE)springer-10.1134/S1070428015010121 
245 0 0 |a Three-component spiro heterocyclization of 1 H -pyrrole-2,3-diones with acetonitriles and 4-hydroxycoumarin. Crystal and molecular structure of ethyl 2-amino-3-cyano-1′-cyclohexyl-2′,5-dioxo-5′-phenyl-1′,2′-dihydro-5 H -spiro-[pyrano[3,2- c ]chromene-4,3′-pyrrole]-4′-carboxylate  |h [Elektronische Daten]  |c [M. Dmitriev, P. Silaichev, A. Maslivets] 
520 3 |a Ethyl 4,5-dioxo-2-phenyl-4,5-dihydro-1H-pyrrole-3-carboxylates reacted with malononitrile (methyl cyanoacetate) and 4-hydroxycoumarin to produce substituted ethyl 2-amino-2′,5-dioxo-5′-phenyl-1′,2′-dihydro-5H-spiro[pyrano[3,2-c]chromene-4,3′-pyrrole]-4′-carboxylates. The crystal and molecular structure of ethyl 2-amino-3-cyano-1′-cyclohexyl-2′,5-dioxo-5′-phenyl-1′,2′-dihydro-5H-spiro[pyrano[3,2-c]chromene-4,3′-pyrrole]-4′-carboxylate was determined by X-ray analysis. 
540 |a Pleiades Publishing, Ltd., 2015 
700 1 |a Dmitriev  |D M.  |u Perm State National Research University, ul. Bukireva 15, 614990, Perm, Russia  |4 aut 
700 1 |a Silaichev  |D P.  |u Perm State National Research University, ul. Bukireva 15, 614990, Perm, Russia  |4 aut 
700 1 |a Maslivets  |D A.  |u Perm State National Research University, ul. Bukireva 15, 614990, Perm, Russia  |4 aut 
773 0 |t Russian Journal of Organic Chemistry  |d Pleiades Publishing  |g 51/1(2015-01-01), 74-77  |x 1070-4280  |q 51:1<74  |1 2015  |2 51  |o 11178 
856 4 0 |u https://doi.org/10.1134/S1070428015010121  |q text/html  |z Onlinezugriff via DOI 
898 |a BK010053  |b XK010053  |c XK010000 
900 7 |a Metadata rights reserved  |b Springer special CC-BY-NC licence  |2 nationallicence 
908 |D 1  |a research-article  |2 jats 
949 |B NATIONALLICENCE  |F NATIONALLICENCE  |b NL-springer 
950 |B NATIONALLICENCE  |P 856  |E 40  |u https://doi.org/10.1134/S1070428015010121  |q text/html  |z Onlinezugriff via DOI 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Dmitriev  |D M.  |u Perm State National Research University, ul. Bukireva 15, 614990, Perm, Russia  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Silaichev  |D P.  |u Perm State National Research University, ul. Bukireva 15, 614990, Perm, Russia  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Maslivets  |D A.  |u Perm State National Research University, ul. Bukireva 15, 614990, Perm, Russia  |4 aut 
950 |B NATIONALLICENCE  |P 773  |E 0-  |t Russian Journal of Organic Chemistry  |d Pleiades Publishing  |g 51/1(2015-01-01), 74-77  |x 1070-4280  |q 51:1<74  |1 2015  |2 51  |o 11178