Hydrazinolysis of dimethyl 2-bromo-1-(thietan-3-yl)-1 H -imidazole-4,5-dicarboxylates
Gespeichert in:
Verfasser / Beitragende:
[F. Khaliullin, A. Valieva, G. Magadeeva]
Ort, Verlag, Jahr:
2015
Enthalten in:
Russian Journal of Organic Chemistry, 51/1(2015-01-01), 91-94
Format:
Artikel (online)
Online Zugang:
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| 024 | 7 | 0 | |a 10.1134/S1070428015010157 |2 doi |
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| 245 | 0 | 0 | |a Hydrazinolysis of dimethyl 2-bromo-1-(thietan-3-yl)-1 H -imidazole-4,5-dicarboxylates |h [Elektronische Daten] |c [F. Khaliullin, A. Valieva, G. Magadeeva] |
| 520 | 3 | |a Alkylation of dimethyl 2-bromo-1H-imidazole-4,5-dicarboxylate with 2-chloromethylthiirane gave dimethyl 2-bromo-1-(thietan-3-yl)-1H-imidazole-4,5-dicarboxylate which was oxidized to dimethyl 2-bromo-1-(1-oxo-λ4-thietan-3-yl)- and 2-bromo-1-(1,1-dioxo-λ6-thietan-3-yl)-1H-imidazole-4,5-dicarboxylates. Reactions of the resulting thietanyl-substituted imidazoledicarboxylates with hydrazine afforded 2-bromo-1-(thietan-3-yl)-, 2-bromo-1-(1-oxo-λ4-thietan-3-yl)-, and 2-bromo-1-(1,1-dioxo-λ6-thietan-3-yl)-1H-imidazole-4,5-dicarbohydrazides and the corresponding 1-(thietanyl)-substituted 2-bromoimidazo[4,5-d]pyridazine-4,7(5H,6H)-diones. | |
| 540 | |a Pleiades Publishing, Ltd., 2015 | ||
| 700 | 1 | |a Khaliullin |D F. |u Bashkir State Medical University, ul. Lenina 3, 450000, Ufa, Bashkortostan, Russia |4 aut | |
| 700 | 1 | |a Valieva |D A. |u Bashkir State Medical University, ul. Lenina 3, 450000, Ufa, Bashkortostan, Russia |4 aut | |
| 700 | 1 | |a Magadeeva |D G. |u Bashkir State Medical University, ul. Lenina 3, 450000, Ufa, Bashkortostan, Russia |4 aut | |
| 773 | 0 | |t Russian Journal of Organic Chemistry |d Pleiades Publishing |g 51/1(2015-01-01), 91-94 |x 1070-4280 |q 51:1<91 |1 2015 |2 51 |o 11178 | |
| 856 | 4 | 0 | |u https://doi.org/10.1134/S1070428015010157 |q text/html |z Onlinezugriff via DOI |
| 898 | |a BK010053 |b XK010053 |c XK010000 | ||
| 900 | 7 | |a Metadata rights reserved |b Springer special CC-BY-NC licence |2 nationallicence | |
| 908 | |D 1 |a research-article |2 jats | ||
| 949 | |B NATIONALLICENCE |F NATIONALLICENCE |b NL-springer | ||
| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1134/S1070428015010157 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Khaliullin |D F. |u Bashkir State Medical University, ul. Lenina 3, 450000, Ufa, Bashkortostan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Valieva |D A. |u Bashkir State Medical University, ul. Lenina 3, 450000, Ufa, Bashkortostan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Magadeeva |D G. |u Bashkir State Medical University, ul. Lenina 3, 450000, Ufa, Bashkortostan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Russian Journal of Organic Chemistry |d Pleiades Publishing |g 51/1(2015-01-01), 91-94 |x 1070-4280 |q 51:1<91 |1 2015 |2 51 |o 11178 | ||