Stereoselective syntheses of substituted tert -butyl 3-allyl-4-hydroxypiperidine-1-carboxylate
| LEADER | caa a22 4500 | ||
|---|---|---|---|
| 001 | 605530246 | ||
| 003 | CHVBK | ||
| 005 | 20210128100822.0 | ||
| 007 | cr unu---uuuuu | ||
| 008 | 210128e20150401xx s 000 0 eng | ||
| 024 | 7 | 0 | |a 10.1134/S1070428015040053 |2 doi |
| 035 | |a (NATIONALLICENCE)springer-10.1134/S1070428015040053 | ||
| 245 | 0 | 0 | |a Stereoselective syntheses of substituted tert -butyl 3-allyl-4-hydroxypiperidine-1-carboxylate |h [Elektronische Daten] |c [V. Boev, A. Moskalenko, S. Belopukhov, N. Przheval'skii] |
| 520 | 3 | |a tert-Butyl 3-allyl-4-oxopiperidine-1-carboxylate and its derivatives substituted at the 3-position and in the allylic fragment reacted with L-selectride in anhydrous tetrahydrofuran to give tert-butyl (3R,4S)-3-allyl-4-hydroxypiperidine-1-carboxylates (cis isomers) in quantitative yield. The Mitsunobu reaction of the latter with formic or benzoic acid, followed by alkaline hydrolysis, afforded the corresponding trans (3R,4R) isomers. | |
| 540 | |a Pleiades Publishing, Ltd., 2015 | ||
| 700 | 1 | |a Boev |D V. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | |
| 700 | 1 | |a Moskalenko |D A. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | |
| 700 | 1 | |a Belopukhov |D S. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | |
| 700 | 1 | |a Przheval'skii |D N. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | |
| 773 | 0 | |t Russian Journal of Organic Chemistry |d Pleiades Publishing |g 51/4(2015-04-01), 493-497 |x 1070-4280 |q 51:4<493 |1 2015 |2 51 |o 11178 | |
| 856 | 4 | 0 | |u https://doi.org/10.1134/S1070428015040053 |q text/html |z Onlinezugriff via DOI |
| 898 | |a BK010053 |b XK010053 |c XK010000 | ||
| 900 | 7 | |a Metadata rights reserved |b Springer special CC-BY-NC licence |2 nationallicence | |
| 908 | |D 1 |a research-article |2 jats | ||
| 949 | |B NATIONALLICENCE |F NATIONALLICENCE |b NL-springer | ||
| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1134/S1070428015040053 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Boev |D V. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Moskalenko |D A. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Belopukhov |D S. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Przheval'skii |D N. |u "Timiryazev Moscow Agricultural Academy” Russian State Agrarian University, Timiryazevskaya ul. 49, 127550, Moscow, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Russian Journal of Organic Chemistry |d Pleiades Publishing |g 51/4(2015-04-01), 493-497 |x 1070-4280 |q 51:4<493 |1 2015 |2 51 |o 11178 | ||