Synthesis and some features of phase behavior of chiral p -alkoxyphenyl glycerol ethers
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| 024 | 7 | 0 | |a 10.1134/S1070428015020116 |2 doi |
| 035 | |a (NATIONALLICENCE)springer-10.1134/S1070428015020116 | ||
| 245 | 0 | 0 | |a Synthesis and some features of phase behavior of chiral p -alkoxyphenyl glycerol ethers |h [Elektronische Daten] |c [R. Fayzullin, O. Antonovich, D. Zakharychev, Z. Bredikhina, A. Kurenkov, A. Bredikhin] |
| 520 | 3 | |a A series of (S)-3-(4-alkoxyphenoxy)propane-1,2-diols was prepared with the enantiomeric excess 86-92% by Sharpless asymmetric dihydroxylation of 1-alkoxy-4-allyloxybenzenes with an AD-mix-β mixture. R-Enantiomers with enantiomeric excess 97-99% and racemic samples were obtained by reaction of sodium p-substituted phenolates with (R)- and rac-3-chloropropane-1,2-diol. The phase behavior of racemates and scalemates in the produced homolog series of glycerol aryl ethers with hydrocarbon substituents of various length was examined by means of thermomicroscopy. The higher memberes of the homolog series of both racemic and scalemic diols undergo at heating an enantiotropic phase transition to a smectic liquid crystal phase. | |
| 540 | |a Pleiades Publishing, Ltd., 2015 | ||
| 700 | 1 | |a Fayzullin |D R. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | |
| 700 | 1 | |a Antonovich |D O. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | |
| 700 | 1 | |a Zakharychev |D D. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | |
| 700 | 1 | |a Bredikhina |D Z. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | |
| 700 | 1 | |a Kurenkov |D A. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | |
| 700 | 1 | |a Bredikhin |D A. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | |
| 773 | 0 | |t Russian Journal of Organic Chemistry |d Pleiades Publishing |g 51/2(2015-02-01), 202-209 |x 1070-4280 |q 51:2<202 |1 2015 |2 51 |o 11178 | |
| 856 | 4 | 0 | |u https://doi.org/10.1134/S1070428015020116 |q text/html |z Onlinezugriff via DOI |
| 898 | |a BK010053 |b XK010053 |c XK010000 | ||
| 900 | 7 | |a Metadata rights reserved |b Springer special CC-BY-NC licence |2 nationallicence | |
| 908 | |D 1 |a research-article |2 jats | ||
| 949 | |B NATIONALLICENCE |F NATIONALLICENCE |b NL-springer | ||
| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1134/S1070428015020116 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Fayzullin |D R. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Antonovich |D O. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Zakharychev |D D. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Bredikhina |D Z. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Kurenkov |D A. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Bredikhin |D A. |u Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Academika Arbuzova 8, 420088, Kazan, Tatarstan, Russia |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Russian Journal of Organic Chemistry |d Pleiades Publishing |g 51/2(2015-02-01), 202-209 |x 1070-4280 |q 51:2<202 |1 2015 |2 51 |o 11178 | ||