Improved Stability and Spectral Quality in Ex Situ Dissolution DNP Using an Improved Transfer Device
Gespeichert in:
Verfasser / Beitragende:
[Sotirios Katsikis, Ildefonso Marin-Montesinos, Miquel Pons, Christian Ludwig, Ulrich Günther]
Ort, Verlag, Jahr:
2015
Enthalten in:
Applied Magnetic Resonance, 46/7(2015-07-01), 723-729
Format:
Artikel (online)
Online Zugang:
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| 024 | 7 | 0 | |a 10.1007/s00723-015-0680-5 |2 doi |
| 035 | |a (NATIONALLICENCE)springer-10.1007/s00723-015-0680-5 | ||
| 245 | 0 | 0 | |a Improved Stability and Spectral Quality in Ex Situ Dissolution DNP Using an Improved Transfer Device |h [Elektronische Daten] |c [Sotirios Katsikis, Ildefonso Marin-Montesinos, Miquel Pons, Christian Ludwig, Ulrich Günther] |
| 520 | 3 | |a Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system. | |
| 540 | |a Springer-Verlag Wien, 2015 | ||
| 700 | 1 | |a Katsikis |D Sotirios |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK |4 aut | |
| 700 | 1 | |a Marin-Montesinos |D Ildefonso |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain |4 aut | |
| 700 | 1 | |a Pons |D Miquel |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain |4 aut | |
| 700 | 1 | |a Ludwig |D Christian |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK |4 aut | |
| 700 | 1 | |a Günther |D Ulrich |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK |4 aut | |
| 773 | 0 | |t Applied Magnetic Resonance |d Springer Vienna |g 46/7(2015-07-01), 723-729 |x 0937-9347 |q 46:7<723 |1 2015 |2 46 |o 723 | |
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| 908 | |D 1 |a research-article |2 jats | ||
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| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1007/s00723-015-0680-5 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Katsikis |D Sotirios |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Marin-Montesinos |D Ildefonso |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Pons |D Miquel |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Ludwig |D Christian |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Günther |D Ulrich |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Applied Magnetic Resonance |d Springer Vienna |g 46/7(2015-07-01), 723-729 |x 0937-9347 |q 46:7<723 |1 2015 |2 46 |o 723 | ||