Improved Stability and Spectral Quality in Ex Situ Dissolution DNP Using an Improved Transfer Device

Verfasser / Beitragende:
[Sotirios Katsikis, Ildefonso Marin-Montesinos, Miquel Pons, Christian Ludwig, Ulrich Günther]
Ort, Verlag, Jahr:
2015
Enthalten in:
Applied Magnetic Resonance, 46/7(2015-07-01), 723-729
Format:
Artikel (online)
ID: 605545553
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024 7 0 |a 10.1007/s00723-015-0680-5  |2 doi 
035 |a (NATIONALLICENCE)springer-10.1007/s00723-015-0680-5 
245 0 0 |a Improved Stability and Spectral Quality in Ex Situ Dissolution DNP Using an Improved Transfer Device  |h [Elektronische Daten]  |c [Sotirios Katsikis, Ildefonso Marin-Montesinos, Miquel Pons, Christian Ludwig, Ulrich Günther] 
520 3 |a Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system. 
540 |a Springer-Verlag Wien, 2015 
700 1 |a Katsikis  |D Sotirios  |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK  |4 aut 
700 1 |a Marin-Montesinos  |D Ildefonso  |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain  |4 aut 
700 1 |a Pons  |D Miquel  |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain  |4 aut 
700 1 |a Ludwig  |D Christian  |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK  |4 aut 
700 1 |a Günther  |D Ulrich  |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK  |4 aut 
773 0 |t Applied Magnetic Resonance  |d Springer Vienna  |g 46/7(2015-07-01), 723-729  |x 0937-9347  |q 46:7<723  |1 2015  |2 46  |o 723 
856 4 0 |u https://doi.org/10.1007/s00723-015-0680-5  |q text/html  |z Onlinezugriff via DOI 
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900 7 |a Metadata rights reserved  |b Springer special CC-BY-NC licence  |2 nationallicence 
908 |D 1  |a research-article  |2 jats 
949 |B NATIONALLICENCE  |F NATIONALLICENCE  |b NL-springer 
950 |B NATIONALLICENCE  |P 856  |E 40  |u https://doi.org/10.1007/s00723-015-0680-5  |q text/html  |z Onlinezugriff via DOI 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Katsikis  |D Sotirios  |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Marin-Montesinos  |D Ildefonso  |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Pons  |D Miquel  |u Biomolecular NMR Laboratory, Organic Chemistry Department, University of Barcelona, Martí i Franquès 1-11, 08028, Barcelona, Spain  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Ludwig  |D Christian  |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Günther  |D Ulrich  |u School of Cancer Sciences, University of Birmingham, Edgbaston, B15 2TT, Birmingham, UK  |4 aut 
950 |B NATIONALLICENCE  |P 773  |E 0-  |t Applied Magnetic Resonance  |d Springer Vienna  |g 46/7(2015-07-01), 723-729  |x 0937-9347  |q 46:7<723  |1 2015  |2 46  |o 723