caa a22 4500 606181717 CHVBK 20210128100812.0 cr unu---uuuuu 210128e20150701xx s 000 0 eng 10.1007/s10876-014-0823-0 doi (NATIONALLICENCE)springer-10.1007/s10876-014-0823-0 Synthesis, Structural Characterization and Thermal Behavior of New Organic-Inorganic Sulfate [Elektronische Daten] [Sami Soukrata, Mohamed Belhouchet, Karim Adil, Tahar Mhiri] The new organic-inorganic compound has been synthesized and characterized by X-ray single crystal, infra-red, Raman spectroscopy and thermal investigations. It crystallizes in the monoclinic space group P21 with following unit cell dimensions: a=4.5542(2)Å, b=10.5171(5)Å, c=13.7373(6)Å, β=93.936(2)°, Z=2 and V=656.42(5)Å3. The crystal structure has been determined and refined to R1=0.0395 and wR2=0.1143 using 3950 independent reflections. The atomic arrangement is defined by infinite anionic chains running parallel to the [100] direction. These last are interconnected to the organic cation by hydrogen bonds N-H O to form a one dimensional network. Springer Science+Business Media New York, 2014 Inorganic compounds nationallicence Chemical synthesis nationallicence Crystal structure nationallicence NMR spectroscopy nationallicence Thermal analysis nationallicence Soukrata Sami Laboratoire Physico-Chimie de l'Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisie aut Belhouchet Mohamed Laboratoire Physico-Chimie de l'Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisie aut Adil Karim Laboratoire des Oxydes et Fluorures, UMR 6010 CNRS, Faculté des Sciences et Techniques, Université du Maine, Avenue O. Messiaen, 72085, Le Mans Cedex 9, France aut Mhiri Tahar Laboratoire Physico-Chimie de l'Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisie aut Journal of Cluster Science Springer US; http://www.springer-ny.com 26/4(2015-07-01), 1413-1424 1040-7278 26:4<1413 2015 26 10876 https://doi.org/10.1007/s10876-014-0823-0 text/html Onlinezugriff via DOI BK010053 XK010053 XK010000 Metadata rights reserved Springer special CC-BY-NC licence nationallicence 1 research-article jats NATIONALLICENCE NATIONALLICENCE NL-springer NATIONALLICENCE 856 40 https://doi.org/10.1007/s10876-014-0823-0 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Soukrata Sami Laboratoire Physico-Chimie de l'Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisie aut NATIONALLICENCE 700 1- Belhouchet Mohamed Laboratoire Physico-Chimie de l'Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisie aut NATIONALLICENCE 700 1- Adil Karim Laboratoire des Oxydes et Fluorures, UMR 6010 CNRS, Faculté des Sciences et Techniques, Université du Maine, Avenue O. Messiaen, 72085, Le Mans Cedex 9, France aut NATIONALLICENCE 700 1- Mhiri Tahar Laboratoire Physico-Chimie de l'Etat Solide, Département de Chimie, Faculté des Sciences de Sfax, Université de Sfax, 3018, Sfax, Tunisie aut NATIONALLICENCE 773 0- Journal of Cluster Science Springer US; http://www.springer-ny.com 26/4(2015-07-01), 1413-1424 1040-7278 26:4<1413 2015 26 10876